Item

Condition

GC-MS model

Agilent 7890A GC/EI/MSD (Agilent 5975 C)

Column

HP 5 MS (5% Phenyl methyl siloxane 30 m, 250 μm)

Detector temperature

280˚C

Oven temperature condition

40˚C (5 min), 5˚C/min, 240˚C (10 min)

Carrier gas

He 9 kPa, 1.5 mL/min

Injection amount

1.0 μl